多晶硅生产中残液搅拌罐密封结构的改造

在处理多晶硅生产中产生的残液时,残液搅拌罐填料密封出现泄漏,针对此问题提出了优化措施,达到了预期效果。     

Morpholine As a Scaffold in Medicinal Chemistry: An Update on Synthetic Strategies

Morpholine is a frequently used heterocycle in medicinal chemistry and a privileged structural component of bioactive molecules. This is mainly due to its contribution to a plethora of biological activities as well as to an improved pharmacokinetic profile of such bioactive molecules. The synthesis of morpholines is a subject of much study due to their biological and pharmacological importance, with the last such review being published in 2013. Here, an overview of the main approaches toward morpholine synthesis or functionalization is presented, emphasizing on novel work which has not been reviewed so far. This review is an update on synthetic strategies leading to easily accessible libraries of bioactives which are of interest for drug discovery projects.     

珲春地区高瓦斯矿井煤自然发火标志气体研究

为了探究珲春地区高瓦斯矿井煤自然发火情况，选取该地区板石煤矿22、23a和八连城煤矿18#、26#共4个煤层进行程序升温特性实验，分析了CO及烃类气体产生量随温度的变化规律，优选自然发火标志气体，测算煤自燃临界温度。结果表明，板石22、23a和八连城18#、26#四个煤层的自燃临界温度分别为101.0℃、97.6℃、121.0℃、169.1℃。CO和C2H4的初现温度大约在30℃与80～120℃，且产生量随温度单调递增，可作为煤自燃预测预报的主要参考指标|而同时，为了保证检测的全面与准确，还可以将规律性良好的其他烃类气体、烯烷比和链烷比进行辅助参考。     

Physical and thermal properties of l‐lactide/ϵ‐caprolactone copolymers: the role of microstructural design

Understanding the underlying role of microstructural design in polymers allows for the manipulation and control of properties for a wide range of specific applications. As such, this work focuses on the study of microstructure–property relationships in l‐ lactide/?‐caprolactone (LL/CL) copolymers. One‐step and two‐step bulk ring‐opening polymerization (ROP) procedures were employed to synthesize LL/CL copolymers of various compositions and chain microstructures. In the one‐step procedure, LL and CL were simultaneously copolymerized to yield P(LL‐stat‐CL) statistical copolymers. In the two‐step procedure, poly(l‐ lactide) (PLL) and poly(?‐caprolactone) (PCL) prepolymers were synthesized in the first step before CL and LL respectively were added in the second step to yield P[LL‐b‐(CL‐stat‐LL)‐b‐LL] and P[CL‐b‐(LL‐stat‐CL)‐b‐CL] block copolymers as the final products. The findings reveal that, in addition to the copolymerization procedure employed, the length and type of the prepolymer play important roles in determining the chain microstructure and thereby the overall properties of the final copolymer. Moreover, control over the degree of crystallinity and the type of crystalline domains, which is controlled during the polymer chemistry process, heavily influences the physical and mechanical properties of the final polymer. In summary, this work describes an interesting approach to the microstructural design of biodegradable copolymers of LL and CL for potential use in biomedical applications. © 2019 Society of Chemical Industry     

印尼BAYAH电厂一次风机故障原因分析与处理

本文针对印尼BAYAH电厂一次风机设备故障，详细的分析了故障产生的原因，介绍了三点法找转子动平衡和工装车削式在线修复电机滑环工法，阐述了两种工法的原理以及实施步骤。     

高精度多环片自动装配控制技术

为了实现对微小环片零件的自动化装配,搭建了自动装配系统.通过4根直线导向轴与4个直线轴承来提高系统的导向精度和刚度.采用直线导轨进行各装配作业模块之间的切换,保证了微小环片零件的自动装配与取出.在环片的装配方向上,螺旋升降机和光栅尺实现环片的位置精度控制.在Lab VIEW编程环境中,采用分层软件架构和模块化控制思想,避免了不必要的数据循环检测与丢失,能够达到环片组件的装配精度要求.控制系统分为系统初始化模块、参数设置模块、装配模块和取出模块,自动装配系统通过各个模块间的相互交流配合完成装配任务.采用本文中自动装配系统装配环片的实验结果表明,环片零件装配的最大位置误差为26μm,垂直度误差为17μm,平均装配时间为75 s/片,可满足环片组件所需的精度要求.     

磁环表面缺陷图像分割算法的研究及实时实现

为实现小型磁环表面细微缺陷图像无监督分割,并提高分割精度与计算效率,本文提出了一种基于改进2D Gabor滤波器组的自适应阈值分割方法。首先,利用多尺度、多方向的Gabor滤波器组对缺陷图像进行滤波降噪处理,抑制目标区域与背景区域内部的噪声污染,同时增强区域间的差异性；然后,通过对处理后图像的灰度统计特性分析,根据缺陷图像的灰度均值及方差构造了灰度阈值计算公式,实现了小型磁环表面细微缺陷图像的自适应分割。实验结果表明,本文算法可快速、准确地分割缺陷并抑制噪声干扰,在分割精度、计算效率等方面也优于传统的选择迭代法、OTSU、最大熵等方法,并能够在先进的SEED-DVS8168平台上实时实现,验证了此算法的可行性与实时性。     

Cutter mark cross method for improvement of contact stiffness by controlling distribution of real contact area

Contact surfaces do not make contact perfectly because such surfaces have a lot of asperities. The real contact area is much smaller than the nominal contact area, and the real contact areas has a non-uniform distribution because of the waviness in the contact surface. The contact stiffness is influenced not only by the deformation of the asperities, but also by the distribution of the real contact areas. In general, a contact surface with a uniform distribution of the real contact areas has greater contact stiffness. However, this requires a grinding finish and costs more than the cutting finish. In this study, a method for uniformly distributing the real contact areas easily, is proposed to improve the contact stiffness of a contact surface finished by cutting. The method is called the cutter mark cross (CMC) method. The allowable waviness in the CMC method is shown. In addition, the effect of the CMC method is investigated by experimentation. The results show that the real contact areas can be distributed uniformly using the CMC method. The horizontal and vertical contact stiffness can also be improved.     

大水深测量校正方法研究与应用

水库水深测量精度直接关系到水库的防洪安全与蓄水兴利。现有回声测深仪无法应对大水深施测的情况，且测量受到水库水温分层影响。利用回声测深仪配合校正标进行大水深测量的校正方法，能够精确检测到回声测深仪水深测量的误差及差值、系统延时问题等，通过与各级校正标的真值比较、修正，能使测值近似真值,且使误差控制在容许范围内。介绍了水深校正标基本原理、操作方法和步骤以及在水库测深中的应用。